Madras Agricultural Journal
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Research Article | Open Access | Peer Review

Hydrodistillation and Soxhlet Method of Extraction and Analyses of Chemical Composition of Citrus Peel Essential Oil

Aruna T Hemalatha G Vellaikumar S Kanchana S Kumutha K
Volume : 109
Issue: Special
Pages: 12 - 18
Downloads: 0
Published: December 22, 2022
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Abstract


The peel which is the primary waste of citrus fruit processing is usually discarded. But these peels are good source of pectin, phenols, flavonoids, and limonene. The peel can be used to extract essential oil that can be used in food system. The present study aimed to extraction and analyse the chemical composition of citrus peel essential oil by hydrodistillation and soxhlet methodThe optimum condition for essential oil extraction by hydrodistillation method was standardized and the oil extraction was efficient at 95 °C. The extraction time was 3 hours with solid solvent ratio of 1:10 (g sample/mL of water). d-Limonene is the major compound present in all three citrus peel essential oils extracted by both the methods followed by β myrcene, α pinene, β pinene, and γ terpinene. Essential oil from fresh citrus peel contains many other compounds such as neral, caryophyllene, β bisbolene, etc. These bioactive volatile compounds are responsible for the antioxidant and antimicrobial properties of the essential oil.

DOI
Pages
12 - 18
Creative Commons
Copyright
© The Author(s), 2025. Published by Madras Agricultural Students' Union in Madras Agricultural Journal (MAJ). This is an Open Access article, distributed under the terms of the Creative Commons Attribution 4.0 License (http://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution and reproduction in any medium, provided the original work is properly cited by the user.

Keywords


Citrus peel; Essential oil; Hydrodistillation; Soxhlet extraction; Limonene
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