Madras Agricultural Journal
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Research Article | Open Access | Peer Review

Simple and Rapid Method for Determination of Flubendiamide and its Residues in Soil and Water by HPLC-UV Detection

Volume : 99
Issue: Apr-jun
Pages: 352 - 355
Published: May 03, 2023
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Abstract


A simple and rapid method for the analysis of flubendiamide and its major metabolite desiodo flubendiamide, in soils and water with acetonitrile and ethyl acetate, respectively, is presented. Quantification was performed by reversed phase HPLC with UV detector. Mean recoveries of flubendiamide and desiodo flubendiamide in soils ranged from 88.01- 90.26 % and 90.5-92.29 % respectively. The applicability of the method to the determination of flubendiamide and desiodo flubendiamide in spiked water at three pH levels (4, 7 and 9.2) was evaluated. Recoveries for flubendiamide and desiodo flubendiamide spiked water were in the ranges 89.21-92.32 % and 92.2-95.57 % respectively. The detector linearity and the repeatability of the method were very precise.

DOI
Pages
352 - 355
Creative Commons
Copyright
© The Author(s), 2025. Published by Madras Agricultural Students' Union in Madras Agricultural Journal (MAJ). This is an Open Access article, distributed under the terms of the Creative Commons Attribution 4.0 License (http://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution and reproduction in any medium, provided the original work is properly cited by the user.

Keywords


Flubendiamide Desiodoflubendiamide HPLC-UV Soil Water.
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